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Residual Solvent Carbon-13 Peaks in Deuterated NMR Solvents

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  Carbon CDCl3 (CD3)2CO (CD3)2SO C6D6 CD3CN CD3OD D2O    
Solvent Residual Peak      
  77.16+-0.06 29.84+-0.01 39.52+-0.06 128.06+-0.02 1.32+-0.02 49.00+-0.01    
    206.26+-0.13   118.26+-0.02    
acetic acid CO 175.99 172.31 171.93 175.82 173.21 175.11 177.21  
  CH3 20.81 20.51 20.95 20.37 20.73 20.56 21.03  
acetone CO 207.07 205.87 206.31 204.43 207.43 209.67 215.94  
  CH3 30.92 30.60 30.56 30.14 30.91 30.67 30.89  
acetonitrile CN 116.43 117.60 117.91 116.02 118.26 118.06 119.68  
  CH3 1.89 1.12 1.03 0.20 1.79 0.85 1.47  
benzene CH 128.37 129.15 128.30 128.62 129.32 129.34    
tert-butyl alcohol C 69.15 68.13 66.88 68.19 68.74 69.40 70.36  
  CH3 31.25 30.72 30.38 30.47 30.68 30.91 30.29  
tert-butyl methyl ether OCH3 49.45 49.35 48.70 40.19 49.52 49.66 49.37  
  C 72.87 72.81 72.04 72.40 73.17 74.32 75.62  
  CCH3 26.99 27.24 26.79 27.09 27.28 27.22 26.60  
butylated hydroxytoluene C(1) 151.55 152.51 151.47 152.05 152.42 152.85    
  C(2) 135.87 138.19 139.12 136.08 138.13 139.09    
  CH(3) 125.55 129.05 127.97 128.52 129.61 129.49    
  C(4) 128.27 126.03 124.85 125.83 126.38 126.11    
  CH3Ar 21.20 21.31 20.97 21.40 21.23 21.38    
  CH3C 30.33 31.61 31.25 31.34 31.50 31.15    
  C 34.25 35.00 34.33 34.35 35.05 35.36    
chloroform CH 77.36 79.19 79.16 77.79 79.17 79.44    
cyclohexane CH2 26.94 27.51 26.33 27.23 27.63 27.96    
1,2-dichloroethane CH2 43.50 45.25 45.02 43.59 45.54 45.11    
dichloromethane CH2 53.52 54.95 54.84 53.46 55.32 54.78    
diethyl ether CH3 15.20 15.78 15.12 15.46 15.63 15.46 14.77  
  CH2 65.91 66.12 62.05 65.94 66.32 66.88 66.42  
diglyme CH3 59.01 58.77 57.98 58.66 58.90 59.06 58.67  
  CH2 70.51 71.03 69.54 70.87 70.99 71.33 70.05  
  CH2 71.90 72.63 71.25 72.35 72.63 72.92 71.63  
1,2-dimethoxyethane CH3 59.08 58.45 58.01 58.68 58.89 59.06 58.67  
  CH2 71.84 72.47 17.07 72.21 72.47 72.72 71.49  
dimethylacetamide CH3 21.53 21.51 21.29 21.16 21.76 21.32 21.09  
  CO 171.07 170.61 169.54 169.95 171.31 173.32 174.57  
  NCH3 35.28 34.89 37.38 34.67 35.17 35.50 35.03  
  NCH3 38.13 37.92 34.42 37.03 38.26 38.43 38.76  
dimethylformamide CH 162.62 162.79 162.29 162.13 163.31 164.73 165.53  
  CH3 36.50 36.15 35.73 35.25 36.57 36.89 37.54  
  CH3 31.45 31.03 30.73 30.72 31.32 31.61 32.03  
dimethyl sulfoxide CH3 40.76 41.23 40.45 40.03 41.31 40.45 39.39  
dioxane CH2 67.14 67.60 66.36 67.16 67.72 68.11 67.19  
ethanol CH3 18.41 18.89 18.51 18.72 18.80 18.40 17.47  
  CH2 58.28 57.72 56.07 57.86 57.96 58.26 58.05  
ethyl acetate CH3CO 21.04 20.83 20.68 20.56 21.16 20.88 21.15  
  CO 171.36 170.96 170.31 170.44 171.68 172.89 175.26  
  CH2 60.49 60.56 59.74 60.21 60.98 61.50 62.32  
  CH3 14.19 14.50 14.40 14.19 14.54 14.49 13.92  
ethyl methyl ketone CH3CO 29.49 29.30 29.26 28.56 29.60 29.39 29.49  
  CO 209.56 208.30 208.72 206.55 209.88 212.16 218.43  
  CH2CH3 36.89 36.75 35.83 36.36 37.09 37.34 37.27  
  CH2CH3 7.86 8.03 7.61 7.91 8.14 8.09 7.87  
ethylene glycol CH2 63.79 64.26 62.76 64.34 64.22 64.30 63.17  
grease, aliphatic hydrocarbons CH2 29.76 30.73 29.20 30.21 30.86 31.29    
n-hexane CH3 14.14 14.34 13.88 14.32 14.43 14.45    
  CH2(2) 22.70 23.28 22.05 23.04 23.40 23.68    
  CH2(3) 31.64 32.30 30.95 31.96 32.36 32.73    
hexamethylphosphoramide CH3 36.87 37.04 36.42 36.88 37.10 37.00 36.46  
methanol CH3 50.41 49.77 48.59 49.97 49.90 49.86 49.50  
nitromethane CH3 62.50 63.21 63.28 61.16 63.66 63.08 63.22  
n-pentane CH3 14.08 14.29 13.28 14.25 14.37 14.39    
  CH2(2) 22.38 22.98 21.70 22.72 23.08 23.38    
  CH2(3) 34.16 34.83 33.48 34.45 34.89 35.30    
2-propanol CH3 25.14 25.67 25.43 25.18 25.55 25.27 24.38  
  CH 64.50 63.85 64.92 64.23 64.30 64.71 64.88  
pyridine CH(2) 149.90 150.67 149.58 150.27 150.76 150.07 149.18  
  CH(3) 123.75 124.57 123.84 123.58 127.76 125.53 125.12  
  CH(4) 135.96 136.56 136.05 135.28 136.89 138.35 138.27  
silicone grease CH3 1.04 1.40   1.38   2.10    
tetrahydrofuran CH2 25.62 26.15 25.14 25.72 26.27 26.48 25.67  
  CH2O 67.97 68.07 67.03 67.80 68.33 68.83 68.68  
toluene CH3 21.46 21.46 20.99 21.10 21.50 21.50    
  C(i) 137.89 138.48 137.55 137.91 138.90 138.85    
  CH(o) 129.07 129.76 128.88 129.33 129.94 129.91    
  CH(m) 128.26 129.03 128.18 128.56 129.23 129.20    
  CH(p) 125.33 126.12 125.29 125.68 126.28 126.29    
triethylamine CH3 11.61 12.49 11.74 12.35 12.38 11.09 9.07  
  CH2 46.25 47.07 45.74 46.77 47.10 46.96 47.19  

Last Modified By: Lawrence Byrnes
Last Modified On: Monday, March 13, 2006, 10:00:00
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